hay all,
i made the precipitate according to
this method
i did not precipitate it with NaOH, i just let all the H2O2 evap off, this would leave a very fluffy and light White powder,
i baked this precipitate in in a oven pan with lid
some water vapor came of it and slowly escaped true the lids opening (its not air tight)
this would in time leave a gray to brown white powder. this powder is not water soluble,
after washing it with some distilled water, i set it in the oven pan again, with some more distilled water, and i put the lid on it..
now slowly heating this and forming a miniature biosphere, this would evap the water up and condense it again and dropping the bottom again, i did this for some time about 2 days after that i left it for 3-4 days. now most of the precipitate hes dissolved again...
way this happens i dont know but i think its a good sign hehe..
i am heating it again with some candle fire now and see if the rest will dissolve again, if so, i will evap the water and see what is left behind.
i will add some photos soon so it is some what more clear what is happening and what i am using.
with love...
Panoramix